Extraction 1st time alcohol extraction info and advice

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im just about to try my first alcohol extraction i want to make a tincture, strong as possible with what i have so that i wont have to take much for a dose as i dont really like booze.
im on a tolerance/sickness break at the moment so less chance of me getting stoned and screwing this up :thumbs: hopefully anyway

to work with i have a 50cl (~18oz) bottle of poteen (basically moonshine) liquor 90% volume 180 proof, 15 grams of easy ryder that i took probably a week early as it was underwatered and as much as i need from a few other strains if needed.

ive been looking around the net for different recipes and so far this seems to be the best put together ones i have found but obviously i dont know if they are or not so im asking which would be best or for an alternative.

i am also happy to try a few different recipes maybe 2 or 3 anyway so whichever seems easiest/stongest with what i have.

also recipes seem split on cooking before or reducing after or nothing atall. which gets best results.. time is not really an issue though i would like to try something in the next few months so i was thinking maybe one short method like the first and one long (shaking bottle in the dark for months.


way too much to read probably but any help is appreciated id like to get started in the next few days so if i dont hear anything ill just try a few that i think sound good.

as ive said i dont know if these are useful so sorry for any misinformation posted but there arent too many threads on here with info (that i could find atleast) so maybe this will help someone anyway.
also i dont know who these are by as they are copy+pasted from many different sites.

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"The Definitive Green Dragon (Cannabis Tincture)
Here is the very successful result of a considerable amount of research into the elusive and magical Green Dragon.

This is a simple and efficient 4 Step process.

Ingredients:
1/8oz high quality cannabis
2 oz Bacardi Rum – 151 proof


Process Summary:

1. Chop cannabis very fine (coffee grinder works great)

2. Place in a shallow pan (pie pan with aluminum foil works great) and bake at 325°F for 4-5 minutes.

3. Remove from oven and place cannabis and place in 2 oz of rum (use a small wide mouth mason jar)

4. Simmer in a water bath for 20 minutes. Maintain temperature of the rum/cannabis mixture between 150°F – 165°F.

5. Strain the mixture and store.


Dosage:
One eyedropper is very nice. Two puts you in space. But you should self-titrate. Effects take about 1.5 hours to begin (at least in myself) and lasted for 5 hours (1 dropper) to 7-8 hours (2 droppers).


Process details—references and rationalizations:
1. Chop the cannabis—more surface area gives means a faster and more efficient extraction.

2. Bake the cannabis.
In whole-plant cannabis, THC content is expressed as THCA (tetrahydrocannabolic acid) prior to decarboxylation into THC, which takes place when cannabis is heated during cooking, and smoked or vaporized ingestion. THCA is a mild analgesic and anti-inflammatory but does not have good affinity with our CB1 receptors, so in order to make a THC-rich tincture that has many of the same therapeutic effects as smoked ingestion (including rapid absorption, quick relief and ease of self-titration), we must convert the THCA in the plant matter into THC prior to extracting it through an alcohol soak. (from Vancouver Island Compassion Society http://thevics.com/cannamist.htm)
THC vaporizes at about 380°F. We want to heat the cannabis to convert THCA to THC, but keep the temperature under 380°F. That is why 325°F is used. Between four and five minutes your oven (and house) will start to smell very strong. This is the time to remove the cannabis from the oven.

Notice also that there is considerable misinformation regarding heating the cannabis. It is true that you don't have to heat it to extract both THC and THCA, but the amount of THC in whole plant preparations is relatively small compared to after decarboxylation of the THCA. So if you want to maximize the strength of your tincture you must heat the cannabis prior to extraction.

3. Use the highest proof alcohol available. In my area this was Bacardi 151. The more alcohol the more efficient the extraction will be.

4. Simmer the mixture.
This is one of the areas that seems to be most debated. Many recipes call for placing the cannabis (unbaked of course) into the alcohol and waiting 2 – 6 weeks. The main concern with heating the alcohol is that it is “explosive” (not exactly true...it is however flammable).

The purpose of the simmering is to heat the alcohol mixture to improve extraction rates and efficiencies. Heating during extraction increases the motion of the molecules (basic physics/chemistry) and drastically decreases extraction times. The boiling point of pure ethanol is 173°F (78°C). We will use the water bath to heat the rum/cannabis mixture to just below the boiling point of ethanol.

Heating the alcohol mixture can be done very safely using a hot water bath. You will need an accurate candy or quick read thermometer. Place about 1 inch of water in a wide, vertical-edged pan (9” wide x 3” high). Bring the water to a low simmer. The rum/cannabis mixture should be in a small (1 pint) mason jar. Do NOT cover the jar.

Put the thermometer into the mason jar and place into the simmering water bath. Bring the temperature of the rum/cannabis mixture to about 165°F (I maintain it between 150°F and 165°F). You want the alcohol mixture to be just barely moving (not boiling, but showing active convection within the mixture). If the mixture starts to bubble too much, just turn down the water bath.

You should have the oven fan on high. You will notice that any alcohol fumes are mixed with water vapor from the water bath and vented out the fan. This combined with the fact that you are trying not to boil the ethanol makes the process quite safe.

5. Strain, titrate, and store.
When you are finished with the extraction you will be left with about 1oz of green dragon tincture. Note that one ounce of the alcohol has evaporated.

Now you should test your eyedropper. In my test 34 full droppers equaled one ounce of liquid (this is a little less than one gram of liquid per dropperful as 29g equals 1ounce).

The liquid should be dark green and smell like cannabis.

6. Dosage.
Everybody is probably different. It takes me 1.5 hours to feel the effects of eating cannabis. Similarly this tincture also takes 1.5 hours to take effect.

I had tried a tincture someone had made using the cold extraction method with the same amount of cannabis and found that 5 droppers did pretty much nothing.

Using my Green Dragon technique I find that one dropper will bring effects on in 1.5 hours and last 5 hours with 1.5 hours of lingering aftereffects.

Two droppers gave me a "spiritual dose" (as strong as any brownie I ever had). Effects lasted 7-8 hours with lingering effects for 2 more hours.

This means that 1/8oz of good cannabis yields about 30-34 doses of tincture (1 dropperful is really all I need). And is much more pleasant than smoking (which really is bad for you and your lungs and the reason I've stopped smoking entirely).

===============================================
Aye mates. Been seeing lots of Green Dragon threads lately, thought why not just do a big thread on it instead of answering it over and over again. Ive done lots and lots of cooking involving THC, yet one style stands out from all of them. Ingesting THC by way of alcohol. When many people think of green dragon, they think of a drink that can get them stoned. End of story. When I think of it, I see endless possibilities. First Ill start by giving a detailed instruction for making the basic cookie cutter Green Dragon drink. Then I will go into details on how to experiment around with it.

The basic recipe is such as this:

Materials:

400 mL Vodka (Anything Higher than 40% Alc)
~6.5g Bud (For .7g Per Shot - If This Is Too Much For You, Lower It)
Mason Jar

Optional Prep - The taste of Green Dragon is not a great taste in particular. This taste can be reduced quite well by watercuring your bud for a day. Watercuring consists of completely submerging your bud, unground, in water. It is not to be covered as evaporation is good. Do this for a day or so, maybe two. The whole week is not needed for watercuring. After this, you can shake excess water off the buds and put them right into the vodka. If the bud isnt completely submerged, it will mold. You dont want this to be ground. Whole buds work much better. Then grind them for the actual procedure.

Procedure:

1. Add Ground Cannabis to Jar

2. Pour in 400mL Vodka into Jar

3. Close Jar and Shake - Put the jar somewhere you are near often so you can give a good shaking whenever you pass it etc. Keep doing this for about 3 weeks. Many people say for 2 months, however this is more time than necessary. As long as you shake it anyway.

4. Optional - Boil a pot of water and put the mason jar into it with the cap off. Leave for a couple of minutes, you dont want it to be on extreme heat, maybe 4-5 out of ten heat settings. You can have it on high to boil it then turn it back down once you put the jar it. This adds a bit of potency by converting the THCA to THC inside the buds, releasing the COOH from the compound. The added potency will not make a dramatic difference however you are making sure your bud is getting used for all its worth. Some alcohol will boil off resulting in a more concentrated mixture, just remember that this recipe is targeted for a shot a dose. You may want to use less if a lot of alcohol boils off.

5. Strain and enjoy!
================================================

grow weeds coming from
hxxps://www.autoflower.org/f43/first-auto-grow-t5s-3095-7.html

if theres any difference between methods in resulting effect(i doubt there is much) i would probably prefer a cerebral trippy high but doesnt matter anyway i enjoy it all.

would water curing help with anything?

any help appreciated.
thanks.
 

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Nice thread bgrt,

I have allways wondered how to do this properly.. Many thanks..
I made some butane honey oil this year, I reckon you could use a strong alcohol to break it down, iv never tried it so could be wrong, but if it worked that would be some killer stuff.. Im gonna try this after my current grow, nothing compares to the strength of b.h.o..

Peace..
 
hey thanks TBM yeh i couldnt find any two recipes that matched up so any corrections from your experience are appreciated, i just copied and pasted these two so the bacardi is from whoever wrote the recipe.

i will be using that poteen 90% 180 proof stuff, its quadruple distilled and smells not too harsh id say it wont be too bad but i probably will flavour it after.
ive seen some people saying star anise seeds for a liquorice flavour i wouldnt mind that or citrus like you were saying and some other things.

i would like to keep this for as long as possible as i already have like 2lb of budder and enough to smoke for a while would coconut oil affect the shelf life?

i have a ricer from making butter anyway so theres one thing off the list.
is sublingualy a good way to take it (under the tongue if i have the word wrong) i have read some people saying this is stupid i was just going to put a dropper full in a drink or food etc anyway but just curious.

just got a crock pot anyway 1 more thing down.*where do you buy glycerine? and i have never seen coconut oil. health food shops? world food kinda places?
to p.l.u.r. yeh im a little wary with butane extraction as im only starting out. im thinking ill start with the safest (imo) and someday ill get the balls to try that :P im not sure if i could get any clean butane here anyway shops are devoid of anything ive seen in recipes to make anything like this. have to order in stuff probably

ill post results good or bad anyway.
 
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so i have looked everywhere in my town for any form of glass thermometer and there is nothing in this backwards hole. so i will not be able to measure the temp. my slow cooker has three settings low, high and warm.
found this but im wondering is this a standard thing that all settings are close enough. also which of these settings would be best id guess low but i dunno.

"it's a good idea to cook on HIGH for the first hour to quickly bring the temperature up to 140 degrees. Then turn the dial to LOW and finish cooking. The LOW setting is about 200 degrees, and the HIGH setting is about 300 degrees. "

i only have a metal coil wall thermometer a baby thermometer and a digital thermometer. hopeing i can get something of a reading off one of these somehow.

what would be best? ill probably try it on low unless that turns out to be luke warm anwyay if i dont hear anything. is there a too long to cook for aswell? or should i just let it go 4 or more hours to try and get everything out(unless this only gets more plant matter broken down).

im going to use a small amount the first tiem anyway and see how it goes. scale up if it is good.
advise me before i screw up people! :no:
 
haha yeh i dont think that route is for me either but good to know!

i think ill make a small batch tonight anyway and see how it is and go scouring for glycerine and coco oil soon.
im not in the us and shops here are pretty useless.

cheers for the info ill be back with results good or bad.
 
This is all very good information! Im actually getting ready to make my first tincture tomorrow. Im trying buddah mans method. It seems pretty easy and i like the idea of sweetners, ive not seen that before.
 
I would start off the slow cooker on high to get the temps up, then switch to low. If you're going to leave it for a few hours alone or overnight, might want to switch to warm so it doesn't overcook (basically dry everything out)

think ill do it tomorrow night i got some coffee filters other than that i was probably gonna try a fine sieve but im sure this would be alot better.
ill be watching it like a hawk, i dont sleep much so ill make sure it doesnt get too hot.

thanks for the help
 
The rectal may be good for extreem cases of nausea (when someone can't orally injest something). Before IV fluids were commonly used, the rectal method was a standard method of rehydration.
 
If you have never had "greendragon" before... and were one of those guys who said "cookies dont get me high" get ready for something totaly different. The dragon is super high powered, can easly ruin your day, and in some cases can make some have to go to the ER as its that powerfull, so don't fuck around this is the most potent way to ingest MJ. Start with a low dose and work your way up.

This aint your girlfriends cookie.
 
so i did it last night anyway, testing tonight. i used around 12oz of that poteen with 15 grams of 3 different strains(RRF, Easyryder, Northern lights bagseed) just bits left around and that one i underwatered and took early.

ground the weed, then put in the oven at around 118c for 30 mins, smelled amazing.

then into the water bath with the booze. added about half of each and let it reduce over a few hours, added again and repeated.

then i strained the mulch through coffee filters pushing out as much as i could when needed then restrained slowly and just left that for 20 mins or so till it was all gone through.

looks pretty nice and doesnt smell too rough but only time will tell.
nearly had a very silly accident though... had it draining into a glass very similar to one i was drinking some coke from and they looked identicle in amount at one point. just on autopilot grabbed it and had it upto my mouth i stopped when i smelt it but that could have been very very bad.. :no: one huge gulp im assuming would take me to space.

anyway my stupidity aside...

i got 2oz~ of this looks so im hoping itll only take a few drops and will last me a long time.
any guesses on dosage TBM? based on what i put in.

can someone tell me the shelflife of something like this if stored in the fridge?
id assume with the alcohol itll keep but not sure.
ill report back with testing.
enjoy the blurry not great pics
 

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